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The developed co-precipitation process recorded maximum chloride removal efficiency in the range of 85-95%. The resultant precipitate i.e., the Friedel's salt was characterized by various techniques such as XRD, XRF and SEM-EDX and confirmed the effective removal of chlorides. The application potential of the process in real iron oxide wash waters with 95% removal efficiency and the possible reusability of precipitate utilizing the "memory effect" of LDHs were found to be highly promising. The study demonstrated the unique application