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In this paper, nanocomposite hydrogel beads were prepared through combining carboxymethyl cellulose (CMC), starch, and ZnO nanoparticles (ZnO-NPs), as well as physical cross-linking with FeCl3. The obtained nanocomposite hydrogel beads were used as a potential candidate for controlled release of anticancer drug doxorubicin (DOX). The nanocomposite hydrogel beads were characterized using FT-IR, XRD, UV-vis, SEM, EDX, TGA and DSC. In addition, gel content, swelling/de-swelling properties, and drug release of the samples were evaluated. The s