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Molybdenum disulfide (MoS2) with a graphite-like layer structure has attracted substantial interest as an anode material for sodium ion batteries (SIBs), but its inherent poor electrical conductivity and slow sodium ion transportation are the two important factors that limit its use in SIBs. Here, we report a general approach to synthesize a series of molecule-intercalated MoS2 with a precisely controlled interlayer distance of 0.62 to 1.24 nm in which the electrical conductivity could be also widely and finely adjusted from 1.3 × 1