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EPR spectroscopy resolves the dissimilar Sb hyperfine tensors of 4, reflecting the inequivalent spin distribution, setting 4 uniquely apart from all previously characterized dipnictene radical anions.We revisit the important issues of polymorphism, structure, and nucleation of cholesterol·H2O using first-principles calculations based on dispersion-augmented density functional theory. For the lesser known monoclinic polymorph, we obtain a fully extended H-bonded network in a structure akin to that of hexagonal ice. We show that the ener