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The slightly better catalytic performance of the 40%Ni-CZO (x = 0.9) could be due to its smaller crystallite size (CZO = 26.83, LSCF = 35.73), rendering more access for the relative gaseous reactants. The best catalyst amongst all was 5%Ni-CZO (x = 0.9), giving 89% toluene conversion, 46% H2 yield, 71% CO selectivity, and 25% CO2 selectivity at optimum reaction temperature of 700 °C.Phosphorus excessively discharged into the water body is a primary cause of eutrophication, but phosphorus resource is limited and non-renewable. If phospho