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Metal-oxide/hydroxide hybrid nanostructures provide an excellent platform to study the interfacial effects on tailoring the catalysis of metal catalysts. Herein, a hybrid nanostructure of Pt@COH)2 supported on SiO2 was synthesized by incipient wetness impregnation of COH)2 with the aid of H2O2 and successive urea-assisted deposition-precipitation of platinum nanoparticles. The Fenton-like reaction between Co2+ and H2O2 during the impregnation process facilitates the formation of active interfacial sites. This hybrid nanostructure exh
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