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Co3O4@rGO were facilely prepared by template free self-assemble in this study. The morphology of Co3O4@rGO was actiniaria-like core-shell structural nanocomposites. The formation mechanism of Co3O4@rGO core-shell nanocomposite was discussed according to its significant time-dependent morphology evolution course. To evaluate the application potential of Co3O4@rGO, its adsorption performance toward highly toxic antimony ions were studied. The Co3O4@rGO nanocomposite exhibit high anti-interference ability and high adsorption ability. The
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