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This multifunctional hydrogel is promising for medication delivery and antimicrobial applications.In this research, poly (mPEGMA-co-MAA) (PA) predicated on monomers of mPEGMA and MAA had been synthesized, and various amino-β-Cyclodextrins with different alkyl chains were conjugated to PA through carbodiimide-mediated coupling responses. The received poly (mPEGMA-co-MAA-g-amino-β-CD) (PA-g-amino-β-CD) ended up being described as FTIR, NMR and TGA. The fluorescence method had been made